Citation: | SHI Jianwei, WU Wei, YANG Huinan, et al. Simultaneous measurement of multi-parameter of liquid film for urea-water-solution by laser spectroscopy[J]. Journal of Beijing University of Aeronautics and Astronautics, 2017, 43(2): 360-365. doi: 10.13700/j.bh.1001-5965.2016.0101(in Chinese) |
Quantitative analysis of liquid film temperature, thickness and mass fraction is extremely crucial to the relevant industrial processes, and these parameters are mutually coupled in the study of the mechanism for heat transfer. Temperature, thickness and mass fraction of liquid film, however, can only be determined individually by conventional measurement techniques. In this paper, a novel measurement method based on Beer-Lambert law to measure the film temperature, thickness and mass fraction of urea-water-solution simultaneously was developed by combining three lasers with different wavelengths:1 420, 1 488 and 1 531 nm. In addition, measurement accuracy of this method was validated by a sample cell with controlled temperature and 1 mm optical path length. The experimental results reveal that average relative errors of thickness, temperature and mass fraction of urea-water-solutions measured by the developed method are 0.51%, 2.59% and 6.32%, respectively.
[1] |
SUN Y Z, SONG X F, JIN M M, et al.Gas-liquid reactive crystallization of lithium carbonate by a falling film column[J].Industrial Engineering Chemistry Research, 2013, 52(49):17598-17606. doi: 10.1021/ie402698v
|
[2] |
PAUTSCH A G, SHEDD T A, NELLIS G F.Thickness measurements of the thin film in spray evaporative cooling[C]//9th Intersociety Conference on Thermal and Thermomechanical Phenomena in Electronic Systems.Piscataway, NJ:IEEE Press, 2004, 1:70-76.
|
[3] |
MAWHINNEY J R, RICHARDSON J K.A review of water mist fire suppression research and development[J].Fire Technology, 1996, 33(1):54-90. https://www.researchgate.net/publication/226216383_A_Review_of_Water_Mist_Fire_Suppression_Research_and_Development_1996
|
[4] |
KAY K Y, ASTERIOS G, RALF Z, et al.Catalyst preparation and deactivation issues for nitrobenzene hydrogenation in a microstructure falling film reactor[J].Catalysis Today, 2003, 81(4):641-651. doi: 10.1016/S0920-5861(03)00162-7
|
[5] |
苏风民, 马鸿斌, 高洪涛, 等.基于薄液膜蒸发的超高速冷冻方法初探[J].工程热物理学报, 2014, 35(3):538-540. http://www.cnki.com.cn/Article/CJFDTOTAL-GCRB201403028.htm
SU F M, MA H B, GAO H T, et al.Preliminary study of ultra-fast cooling methods utilizing thin film evaporation[J].Journal of Engineering Thermophysics, 2014, 35(3):538-540(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-GCRB201403028.htm
|
[6] |
陈世昌, 马建平, 张先明, 等.竖直降液膜流动在反应工程中的应用[J].化工进展, 2014, 33(10):2528-2534. http://www.cnki.com.cn/Article/CJFDTOTAL-HGJZ201410002.htm
CHEN S C, MA J P, ZHANG X M, et al.Advances in application of falling liquid film for reaction engineering[J].Chemical Industry and Engineering Progress, 2014, 33(10):2528-2534(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-HGJZ201410002.htm
|
[7] |
戴干策.化学工程基础:流体流动、传热及传质[M].北京:中国石化出版社, 1991:25-32.
DAI G C.Chemical engineering foundation:Fluid flow, heat transfer and mass transfer[M].Beijing:China Petrochemical Press, 1991:25-32(in Chinese).
|
[8] |
BIRKHOLD F, MEINGAST U, WASSERMANN P, et al.Analysis of the injection of urea-water-solution for automotive SCR DeNOx-systems:Modeling of two-phase flow and spray/wall-interaction:2006-01-0643[R].Warrendale, PA:SAE International, 2006.
|
[9] |
陈冯, 王谦, 何志霞, 等.柴油机尿素Urea-SCR喷射过程参数优化及数值模拟研究[J].内燃机工程, 2015, 36(1): 23-30. http://www.cnki.com.cn/Article/CJFDTOTAL-NRJG201501005.htm
CHEN F, WANG Q, HE Z X, et al.Optimization and numerical simulation of urea spray parameters in diesel engine SCR system[J].Chinese Internal Combustion Engine Engineering, 2015, 36(1):23-30(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-NRJG201501005.htm
|
[10] |
余皎, 王军, 佟德辉, 等.重型柴油机SCR系统布置优化设计[J].内燃机与动力装置, 2010(4):25-29. http://www.cnki.com.cn/Article/CJFDTOTAL-SDNR201004008.htm
YU J, WANG J, TONG D H, et al.Configuration optimization of the SCR system for a heavy duty dieset engine[J].Internal Combustion Engine and Power Plant, 2010(4):25-29(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-SDNR201004008.htm
|
[11] |
喻小伟, 李宇春, 蒋娅, 等.尿素热解研究及其在脱硝中的应用[J].热力发电, 2012, 41(1):1-5. http://www.cnki.com.cn/Article/CJFDTOTAL-RLFD201201002.htm
YU X W, LI Y C, JIANG Y, et al.Study on pyrolysis of urea and its application in denitrifcation[J].Thermal Power Generation, 2012, 41(1):1-5(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-RLFD201201002.htm
|
[12] |
崔洁, 陈雪莉, 王清立, 等.电导法测量新型旋风分离器内液膜的分布规律[J].化工学报, 2009, 60(6):1487-1493. http://www.cnki.com.cn/Article/CJFDTOTAL-HGSZ200906025.htm
CUI J, CHEN X L, WANG Q L, et al.Double-parallel conductance probe for measuring thickness of liquid film in new-type cyclone separator[J].Journal of Chemical Industry and Engineering, 2009, 60(6):1487-1493(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-HGSZ200906025.htm
|
[13] |
张锋, 耿皎, 马少玲, 等.利用电容法测量降膜厚度[J].测量与设备, 2005(4):34-35. http://www.cnki.com.cn/Article/CJFDTOTAL-JLJS200505013.htm
ZHANG F, GENG J, MA S L, et al.Measurement of the falling film thickness by capacitance method[J].Measurement and Equipment, 2005(4):34-35(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-JLJS200505013.htm
|
[14] |
郑丽行, 樊小林, 刘刚, 等.折光率测定尿素含量的方法研究[J].西北农林科技大学学报(自然科学版), 2010, 38(12):93-98. http://www.cnki.com.cn/Article/CJFDTOTAL-XBNY201012017.htm
ZHENG L X, FAN X L, LIU G, et al.Study on refractive index method for determination of urea concentration[J]. Journal of Northwest A & F University (Natural Science Edition), 2010, 38(12):93-98(in Chinese). http://www.cnki.com.cn/Article/CJFDTOTAL-XBNY201012017.htm
|
[15] |
YANG H, GRESZIK D, DREIER T, et al.Simultaneous measurement of liquid water film thickness and vapor temperature using near-infrared tunable diode laser spectroscopy[J].Applied Physics B:Lasers and Optics, 2010, 99(3):385-390. doi: 10.1007/s00340-010-3980-3
|
[16] |
HALBOUT J M, BLIT S, DONADSON W, et al.Efficient phase-matched second-harmonic generation and sum-frequency mixing in urea[J].IEEE Journal of Quantum Electronics, 1979, 15(10):1176-1180. doi: 10.1109/JQE.1979.1069900
|
[17] |
YANG H N, GUO X L, SU M X, et al.Novel method for simultaneous measurement of film thickness and mass fraction of urea-water solution[J].Chinese Optics Letters, 2014, 12(12):123102. doi: 10.3788/COL
|
[18] |
YANG H N, GUO X L, ZHOU W, et al. Investigation on liquid film of urea-water solutions with diode laser absorption spectroscopy[J].Experiments in Fluids, 2015, 56(4):73-1-73-7. doi: 10.1007/s00348-015-1941-7
|