Setup and application of a wetting property measuring instrument
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摘要: 针对复合材料成型工艺的特点,依据毛细原理,研制了浸润性能测试仪.该测试仪包括浸润质量测试系统与温度控制系统,能够定量测试在较宽的温度范围内发生浸润的速率和浸润程度.对该测试仪的准确性与稳定性进行了校准与标定,并运用该仪器研究了纤维种类、树脂粘度和纤维体积含量对树脂/纤维浸润性能的影响规律.研究结果表明该设备为研究各类复合材料中增强材料与基体间的浸润性能提供了方便的测试手段,对指导复合材料制备工艺具有较高的参考价值.Abstract: A new wettablity instrument was developed according to the fabrication characteristic of composites, which could measure the mass increase in fibres penetrated by resins. The instrument was composed of two parts. One was the wicking mass testing system and the other was a temperature-controlled system. It could measure the capillary impregnation of liquids in the fibre bundles with various fibre volume fractions under different temperatures. The instrument was evaluated and adjusted. Based on this, the wetting of resins in glass fibres and carbon fibres were studied. Effects of the type of fibres, the viscosity of resins and the fibre volume fraction on wicking behaviour were also investigated. The results show that this instrument provides a convenient tool for studying on wettability of the reinforced fibres probe by the resin matrix, which is valuable for guiding parameters in the process of composites.
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Key words:
- composite materials /
- wetting /
- fibers /
- testing equipments /
- polymer matrix
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[1] Bismarck A,Kumru M E,Song B,et al. Study on surface and mechanical fiber characteristics and their effect on the adhesion properties to a polycarbonate matrix tuned by anodic carbon fiber oxidation[J] Composites:Part A,1999,30:1351~1366 [2] Taviso Mervi,Kuisma Risto,Pasila Antti,et al. Wetting and wicking of fiber plant straw fractions[J] Industrial Corps and Products, 2003,28:25~35 [3] Rebouillat Serge,Letellier Bertrand,Steffenino Benoit. Wettability of single fibres-beyond the contact angle approach[J] International Journal of Adhesion and Adhesives,1999,19:303~314 [4] 赵振国. 接触角及其在表面化学研究中的应用[J] 化学研究与应用,2000,12(4):370~374 Zhao Zhenguo. Contace angle and its application in surface chemistry research[J] Chemical Research and Application,2000,12(4):370~374(in Chinese) [5] 田 军,徐锦芬,薛群基. 氟聚合物表面接触角滞后的研究[J] 高分子材料科学与工程,1997,9:109~113 Tian Jun,Xu Jinfen,Xue Qunji. Hysteresis study of some fluorine polymer[J] Polymeric Materials Science and Engineering,1997,9:109~113(in Chinese) [6] 汪泽霖. 浅谈树脂对玻璃纤维的浸透性和浸润性[J] 玻璃纤维,1997,5:30~31 Wang Zelin. The discussion of the wetting property and the wetting-out property between resin and glass fiber[J] Glass Fiber,1997,5:30~31(in Chinese) [7] Ahn K J,Seferis James C. Prepreg processing science and engineering[J] Polymer Engineering and Science,1993,33(18):1177~1187 [8] Palmese G R,Karbhari V M. Effects of sizing on microscopic flow in resin transfer molding[J] Polymer Composites,1995,16(4):313~318 [9] Saalbrink A,Lorteije A,Peijs T. The influence of processing parameters on interphase morphology in polymer composites based on phased on phase-separating thermoplastic/epoxy blends[J] Composites Part A,1998,29A:1243~1250
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